JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000956
Submitter
The Noguchi Institute
Reaction ID
R-0000-000956
Regist Date
2012/06/21 16:31:41
REACTANT
MOLECULE ID
JCGG-COM0001085 (Reaction Tree)
Mol
0.642 mmol
MOLECULE ID
JCGG-COM0000047
Reactant Type
Et3N
Mol
1.28 mmol
MOLECULE ID
JCGG-COM0001086
Reactant Type
BzCN (in 7 mL of CH3CN)
Mol
0.706 mmol
MOLECULE ID
JCGG-COM0000057
Reactant Type
MeOH
Volume
5 mL
PRODUCT
MOLECULE ID
JCGG-COM0001087 (Reaction Tree)
Yield
88%
REACTION DETAIL
Reaction Time
10 minutes, 10 minutes
Reaction Temp
0 degree C, NOT specified
Solvent
CH3CN, CH3CN/MeOH
Comment
1) 11+Et3N, BzCN, 2) +MeOH
The reaction temperature of the second phase could not be found.
COMMENT
The PMID could not be found.
There are two phases in this reaction.
REFERENCE
Reference Id
REF-0000-000044
Source
Journal of Carbohydrate Chemistry, 17: 4, 739-758
Doi
10.1080/07328309808002349

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)