JCGG ID |
JCGG-RAC0000954 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-000954 | ||||
Regist Date |
2012/06/21 16:31:36 | ||||
REACTANT | |||||
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|
||||
Mol |
9.18 mmol | ||||
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|
||||
Reactant Type |
NaCNBH3 | ||||
Mol |
91.8 mmol | ||||
|
|
||||
Reactant Type |
HCl (in dry Et2O) | ||||
PRODUCT | |||||
MOLECULE ID |
|
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|||
Yield |
63% | ||||
REACTION DETAIL | |||||
Reaction Time |
2 hours | ||||
Solvent |
dry THF | ||||
Comment |
The reaction temperature could not be found. (considered to be room temp) | ||||
HCl was added dropwise to remain the pH of the solution acidic. | |||||
COMMENT | |||||
The PMID could not be found. | |||||
REFERENCE | |||||
Reference Id |
REF-0000-000044 | ||||
Source |
Journal of Carbohydrate Chemistry, 17: 4, 739-758 | ||||
Doi |
10.1080/07328309808002349 |
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST) |