JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000954
Submitter
The Noguchi Institute
Reaction ID
R-0000-000954
Regist Date
2012/06/21 16:31:36
REACTANT
MOLECULE ID
JCGG-COM0001082 (Reaction Tree)
Mol
9.18 mmol
MOLECULE ID
JCGG-COM0000708
Reactant Type
NaCNBH3
Mol
91.8 mmol
MOLECULE ID
JCGG-COM0000552
Reactant Type
HCl (in dry Et2O)
PRODUCT
MOLECULE ID
JCGG-COM0001084 (Reaction Tree)
Yield
63%
REACTION DETAIL
Reaction Time
2 hours
Solvent
dry THF
Comment
The reaction temperature could not be found. (considered to be room temp)
HCl was added dropwise to remain the pH of the solution acidic.
COMMENT
The PMID could not be found.
REFERENCE
Reference Id
REF-0000-000044
Source
Journal of Carbohydrate Chemistry, 17: 4, 739-758
Doi
10.1080/07328309808002349

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)