Reaction:JCGG-RAC0000944

JCGG ID		JCGG-RAC0000944
Submitter		The Noguchi Institute
Reaction ID		R-0000-000944
Regist Date		2012/06/21 16:31:09
REACTANT
MOLECULE ID		JCGG-COM0001069 (Reaction Tree)
	Mol	0.27 mmol
MOLECULE ID		JCGG-COM0000028
	Reactant Type	BuLi (1.5 M in hexane)
	Mol	0.26 mmol
MOLECULE ID		JCGG-COM0000029
	Reactant Type	ClP(S)Me2
	Mol	0.28 mmol
PRODUCT
MOLECULE ID		JCGG-COM0001070 (Reaction Tree)
	Yield	69%
REACTION DETAIL
Reaction Time		15 minutes, 1.5 hours
Reaction Temp		-30 degree C, -30 degree C
Solvent		dry THF, dry THF
Comment		1) 11+BuLi, 2) +ClP(S)Me2
COMMENT
The PMID could not be found.
There are two phases in this reaction.
REFERENCE
Reference Id		REF-0000-000043
	Source	HETEROCYCLES, Vol. 52, No. 2, 2000, pp. 921-928
	Doi	10.3987/COM-99-S65