JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000940
Submitter
The Noguchi Institute
Reaction ID
R-0000-000940
Regist Date
2012/06/21 16:30:58
REACTANT
MOLECULE ID
JCGG-COM0001062 (Reaction Tree)
Skeleton
JCGG-STR033114
Mol
0.137 mmol
MOLECULE ID
JCGG-COM0001063
Mol
0.41 mmol
MOLECULE ID
JCGG-COM0000531
Reactant Type
H2O
Volume
3 mL
MOLECULE ID
JCGG-COM0000979
Reactant Type
pyridine
Volume
3 mL
PRODUCT
MOLECULE ID
JCGG-COM0001064 (Reaction Tree)
Skeleton
JCGG-STR033114
Yield
69%
REACTION DETAIL
Reaction Time
overnight, 30 minutes
Reaction Temp
room temp, NOT specified
Solvent
pyridine/dioxane = 1mL/3mL, pyridine/dioxane = 1mL/3mL
Comment
1) 7+8, 2) +all the rest
The reaction temperature of the second phase could not be found. (considered to be room temp)
COMMENT
The PMID could not be found.
There are two phases in this reaction.
REFERENCE
Reference Id
REF-0000-000043
Source
HETEROCYCLES, Vol. 52, No. 2, 2000, pp. 921-928
Doi
10.3987/COM-99-S65

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