Reaction:JCGG-RAC0000937

JCGG ID		JCGG-RAC0000937
Submitter		The Noguchi Institute
Reaction ID		R-0000-000937
Regist Date		2012/06/21 16:30:50
REACTANT
MOLECULE ID		JCGG-COM0000863 (Reaction Tree)
	Mol	2.2 mmol
MOLECULE ID		JCGG-COM0000028
	Reactant Type	BuLi (1.68 M in hexane)
	Mol	2.2 mmol
MOLECULE ID		JCGG-COM0000029
	Reactant Type	ClP(S)Me2
	Mol	2.2 mmol
PRODUCT
MOLECULE ID		JCGG-COM0001059 (Reaction Tree)
	Yield	78%
REACTION DETAIL
Reaction Time		15 minutes, 2.5 hours
Reaction Temp		-30 degree C, -30 degree C
Solvent		dry THF, dry THF
Comment		1) 3+BuLi, 2) +ClP(S)Me2
COMMENT
The PMID could not be found.
There are two phases in this reaction.
REFERENCE
Reference Id		REF-0000-000043
	Source	HETEROCYCLES, Vol. 52, No. 2, 2000, pp. 921-928
	Doi	10.3987/COM-99-S65