JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000936
Submitter
The Noguchi Institute
Reaction ID
R-0000-000936
Regist Date
2012/06/21 16:30:47
REACTANT
MOLECULE ID
JCGG-COM0001057 (Reaction Tree)
Mol
0.109 mmol
MOLECULE ID
JCGG-COM0000484
Reactant Type
O3 (gas)
MOLECULE ID
JCGG-COM0000408
Reactant Type
Ph3P
Mol
0.324 mmol
MOLECULE ID
JCGG-COM0000776
Reactant Type
NaBH4
Mol
0.320 mmol
PRODUCT
MOLECULE ID
JCGG-COM0001058 (Reaction Tree)
Yield
95%
REACTION DETAIL
Reaction Time
30 minutes, NOT specified, 1 hour
Reaction Temp
-78 degree C, room temp, 0 degree C
Solvent
CH2Cl2, CH2Cl2, THF
Comment
1) 27+O3, 2) +Ph3P, 3) +NaBH4
The reaction time of the second phase could not be found. (considered to be very short)
COMMENT
The PMID could not be found.
There are three phases in this reaction.
REFERENCE
Reference Id
REF-0000-000042
Source
Tetrahedron 64 (2008) 8082-8088
Doi
10.1016/j.tet.2008.06.068

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)