JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000934
Submitter
The Noguchi Institute
Reaction ID
R-0000-000934
Regist Date
2012/06/21 16:30:42
REACTANT
MOLECULE ID
JCGG-COM0000864 (Reaction Tree)
Mol
0.0736 mmol
MOLECULE ID
JCGG-COM0000439
Reactant Type
allylMgBr (1.0 M in Et2O)
Mol
0.177 mmol
PRODUCT
MOLECULE ID
JCGG-COM0001055 (Reaction Tree)
Yield
85%
MOLECULE ID
JCGG-COM0001056 (Reaction Tree)
Product Type
intermediate
Yield
9%
REACTION DETAIL
Reaction Time
1 hour
Reaction Temp
-78 degree C
Solvent
THF
Comment
AllylMgBr was added dropwise.
COMMENT
The PMID could not be found.
REFERENCE
Reference Id
REF-0000-000042
Source
Tetrahedron 64 (2008) 8082-8088
Doi
10.1016/j.tet.2008.06.068

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)