Reaction:JCGG-RAC0000930

JCGG ID		JCGG-RAC0000930
Submitter		The Noguchi Institute
Reaction ID		R-0000-000930
Regist Date		2012/06/21 16:30:31
REACTANT
MOLECULE ID		JCGG-COM0001050 (Reaction Tree)
	Mol	0.0297 mmol
MOLECULE ID		JCGG-COM0000484
	Reactant Type	O3 (gas)
MOLECULE ID		JCGG-COM0000408
	Reactant Type	Ph3P
	Mol	0.154 mmol
MOLECULE ID		JCGG-COM0000776
	Reactant Type	NaBH4
	Mol	0.293 mmol
PRODUCT
MOLECULE ID		JCGG-COM0001051 (Reaction Tree)
	Yield	77%
REACTION DETAIL
Reaction Time		30 minutes, NOT specified, 2.5 hours
Reaction Temp		-78 degree C, room temp, 0 degree C
Solvent		CH2Cl2, CH2Cl2, THF
Comment		1) 22+O3, 2) +Ph3P, 3) +NaBH4
		The reaction time of the second phase could not be found. (considered to be very short)
COMMENT
The PMID could not be found.
There are three phases in this reaction.
REFERENCE
Reference Id		REF-0000-000042
	Source	Tetrahedron 64 (2008) 8082-8088
	Doi	10.1016/j.tet.2008.06.068