JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000928
Submitter
The Noguchi Institute
Reaction ID
R-0000-000928
Regist Date
2012/06/21 16:30:26
REACTANT
MOLECULE ID
JCGG-COM0001048 (Reaction Tree)
Mol
0.153 mmol
MOLECULE ID
JCGG-COM0000772
Reactant Type
vinylMgCl (1.3 M in THF)
Mol
0.307 mmol
MOLECULE ID
JCGG-COM0000773
Reactant Type
dry CeCl3
Mol
0.250 mmol
PRODUCT
MOLECULE ID
JCGG-COM0001049 (Reaction Tree)
Yield
64%
REACTION DETAIL
Reaction Time
1 hour
Reaction Temp
-78 degree C
Solvent
PhCH3
Comment
vinylMgCl was added dropwise.
COMMENT
The PMID could not be found.
REFERENCE
Reference Id
REF-0000-000042
Source
Tetrahedron 64 (2008) 8082-8088
Doi
10.1016/j.tet.2008.06.068

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)