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Glycan Syntheses |
JCGG ID |
JCGG-RAC0000926 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-000926
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Regist Date |
2012/06/21 16:30:21 | ||||
| REACTANT | |||||
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Mol |
0.0781 mmol | ||||
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Reactant Type |
O3 (gas) | ||||
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Reactant Type |
Ph3P | ||||
Mol |
0.448 mmol | ||||
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Reactant Type |
NaBH4 | ||||
Mol |
0.666 mmol | ||||
| PRODUCT | |||||
MOLECULE ID |
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Yield |
73% | ||||
| REACTION DETAIL | |||||
Reaction Time |
40 minutes, NOT specified, 3 hours | ||||
Reaction Temp |
-78 degree C, room temp, 0 degree C | ||||
Solvent |
CH2Cl2, CH2Cl2, THF | ||||
Comment |
1) 19+O3, 2) +Ph3P, 3) +NaBH4 | ||||
| The reaction time of the second phase could not be found. (considered to be very short) | |||||
| COMMENT | |||||
| The PMID could not be found. | |||||
| There are three phases in this reaction. | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000042 | ||||
Source |
Tetrahedron 64 (2008) 8082-8088 | ||||
Doi |
10.1016/j.tet.2008.06.068 | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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