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Glycan Syntheses |
JCGG ID |
JCGG-RAC0000924 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-000924
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Regist Date |
2012/06/21 16:30:16 | ||||
| REACTANT | |||||
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Mol |
0.153 mmol | ||||
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Reactant Type |
vinylMgCl (1.4 M in THF) | ||||
Mol |
0.307 mmol | ||||
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Reactant Type |
dry CeCl3 | ||||
Mol |
0.307 mmol | ||||
| PRODUCT | |||||
MOLECULE ID |
|
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Yield |
80% | ||||
| REACTION DETAIL | |||||
Reaction Time |
3 hours | ||||
Reaction Temp |
-78 degree C | ||||
Solvent |
THF | ||||
Comment |
vinylMgCl was added dropwise. | ||||
| COMMENT | |||||
| The PMID could not be found. | |||||
| ATTENTION: There is a numerical discrepancy between the scheme and the written method. (the reaction time) | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000042 | ||||
Source |
Tetrahedron 64 (2008) 8082-8088 | ||||
Doi |
10.1016/j.tet.2008.06.068 | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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