JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000922
Submitter
The Noguchi Institute
Reaction ID
R-0000-000912
Regist Date
2012/06/21 16:29:44
REACTANT
MOLECULE ID
JCGG-COM0001039 (Reaction Tree)
Reactant Type
Ac-[Ser(O-hexa saccharide]3-AlaValAlaVal-OH
Mol
1.87 micro mole
MOLECULE ID
JCGG-COM0001040
Reactant Type
Pam3Cys*HOAc
Mol
5.7 micro mole
MOLECULE ID
JCGG-COM0000426
Reactant Type
DIEA
Volume
1 drop (excess)
MOLECULE ID
JCGG-COM0001029
Reactant Type
HOAT
Mol
7.5 micro mole
MOLECULE ID
JCGG-COM0001030
Reactant Type
HATU
Mol
3.7 micro mole
PRODUCT
MOLECULE ID
JCGG-COM0001041 (Reaction Tree)
Yield
32%
REACTION DETAIL
Reaction Time
20 hours
Solvent
DMF
Comment
The reaction temperature could not be found. (considered to be room temp)
COMMENT
The PMID could not be found.
REFERENCE
Reference Id
REF-0000-000041
Source
J. Am. Chem. Soc. 1999, 121, 10636-10637
Doi
10.1021/ja992309s

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