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Glycan Syntheses |
JCGG ID |
JCGG-RAC0000915 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-000917
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Regist Date |
2012/06/21 16:29:57 | ||||
| REACTANT | |||||
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Mol |
0.34 mmol | ||||
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Reactant Type |
NaH | ||||
Mol |
1.4 mmol | ||||
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Reactant Type |
BnBr | ||||
Mol |
0.58 mmol | ||||
| PRODUCT | |||||
MOLECULE ID |
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Yield |
96% | ||||
| REACTION DETAIL | |||||
Reaction Time |
40 minutes, 5+30 minutes, overnight | ||||
Reaction Temp |
0 degree C, 0 degree C, room temp | ||||
Solvent |
anhydrous DMF, anhydrous DMF, anhydrous DMF | ||||
Comment |
1) 11+NaH, 2) +BnBr, 3) temperature change | ||||
| BnBr was added dropwise over a 5-min period. | |||||
| COMMENT | |||||
| The PMID could not be found. | |||||
| There are three phases in this reaction. | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000042 | ||||
Source |
Tetrahedron 64 (2008) 8082-8088 | ||||
Doi |
10.1016/j.tet.2008.06.068 | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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