JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000911
Submitter
The Noguchi Institute
Reaction ID
R-0000-000914
Regist Date
2012/06/21 16:29:49
REACTANT
MOLECULE ID
JCGG-COM0000760 (Reaction Tree)
Skeleton
JCGG-STR032527
Mol
0.21 mmol
MOLECULE ID
JCGG-COM0000761
Reactant Type
Tf2O
Mol
0.32 mmol
PRODUCT
MOLECULE ID
JCGG-COM0000762 (Reaction Tree)
Skeleton
JCGG-STR032527
Yield
93%
REACTION DETAIL
Reaction Time
2.5 hours
Reaction Temp
room temp
Solvent
pyridine
Comment
The reactants were mixed at -20 degree in Celsius, and gradually raised to room temperature within the reaction time.
COMMENT
The PMID could not be found.
REFERENCE
Reference Id
REF-0000-000042
Source
Tetrahedron 64 (2008) 8082-8088
Doi
10.1016/j.tet.2008.06.068

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)