JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
 JCGG-RAC0000888
Submitter
 The Noguchi Institute
Reaction ID
 R-0000-000888
Regist Date
 2012/06/21 16:28:24
REACTANT
MOLECULE ID
 JCGG-COM0000778 (Reaction Tree)
Reactant Type
 glycosyl acetate
Mol
 1 equiv.
MOLECULE ID
 JCGG-COM0000037
Reactant Type
 alcohol
Mol
 1 equiv.
MOLECULE ID
 JCGG-COM0001008
Reactant Type
 YTA
Mol
 0.05 equiv.
PRODUCT
MOLECULE ID
 JCGG-COM0000291 (Reaction Tree)
Skeleton
JCGG-STR032525
Product Type
 alpha
Yield
 22%(alpha/beta=18/82)
MOLECULE ID
 JCGG-COM0000292 (Reaction Tree)
Skeleton
JCGG-STR031569
Product Type
 beta
Yield
 22%(alpha/beta=18/82)
REACTION DETAIL
Reaction Time
 overnight
Solvent
 CH2Cl2
Comment
 The reaction temperature could not be found. (considered to be room temp)
Na2SO4 (Drying Agent) was included in the solvent.
COMMENT
The PMID could not be found.
REFERENCE
Reference Id
 REF-0000-000040
Source
 SYNTHETIC COMMUNICATIONS, 31(6), 899-903 (2001)
Doi
 10.1081/SCC-100103325
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)