JCGG ID |
JCGG-RAC0000873 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-000873 | ||||
Regist Date |
2012/06/21 16:27:43 | ||||
REACTANT | |||||
|
|
||||
Mol |
1 equiv. | ||||
|
|
||||
Reactant Type |
Nucleophile | ||||
Mol |
3 equiv. | ||||
|
|
||||
Reactant Type |
TMSOTf | ||||
Mol |
0.2 equiv. | ||||
PRODUCT | |||||
MOLECULE ID |
|
|
|||
Product Type |
exo-Glucal | ||||
Yield |
39% | ||||
REACTION DETAIL | |||||
Reaction Time |
2 hours | ||||
Reaction Temp |
-40 degree C | ||||
Solvent |
MeCN | ||||
Comment |
Dry CaSO4 was included in the solvent. | ||||
COMMENT | |||||
The PMID could not be found. | |||||
REFERENCE | |||||
Reference Id |
REF-0000-000039 | ||||
Source |
SYNLETT 2007, No. 5, pp 0785-0789 | ||||
Doi |
10.1055/s-2007-970751 |
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST) |