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Glycan Syntheses |
JCGG ID |
JCGG-RAC0000872 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-000872
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Regist Date |
2012/06/21 16:27:41 | ||||
| REACTANT | |||||
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Mol |
1 equiv. | ||||
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Reactant Type |
Nucleophile | ||||
Mol |
3 equiv. | ||||
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Reactant Type |
TMSOTf | ||||
Mol |
0.2 equiv. | ||||
| PRODUCT | |||||
MOLECULE ID |
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Product Type |
exo-Glucal | ||||
Yield |
64% | ||||
MOLECULE ID |
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Product Type |
Ketoside | ||||
Yield |
16% | ||||
| REACTION DETAIL | |||||
Reaction Time |
2 hours | ||||
Reaction Temp |
-40 degree C | ||||
Solvent |
MeCN | ||||
Comment |
Dry CaSO4 was included in the solvent. | ||||
| COMMENT | |||||
| The PMID could not be found. | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000039 | ||||
Source |
SYNLETT 2007, No. 5, pp 0785-0789 | ||||
Doi |
10.1055/s-2007-970751 | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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