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Glycan Syntheses |
JCGG ID |
JCGG-RAC0000868 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-000868
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Regist Date |
2012/06/21 16:27:30 | ||||
| REACTANT | |||||
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Mol |
17 micro mole | ||||
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Reactant Type |
methyl bromoacetate | ||||
Mol |
22 micro mole | ||||
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Reactant Type |
NaH (95% suspension in mineral oil) | ||||
Mol |
2 micro mole | ||||
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Reactant Type |
Bu4NI | ||||
Mol |
8.5 micro mole | ||||
| PRODUCT | |||||
MOLECULE ID |
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Yield |
53% | ||||
| REACTION DETAIL | |||||
Reaction Time |
1 + 4 hours | ||||
Reaction Temp |
room temp | ||||
Solvent |
DMF | ||||
Comment |
The reactants were mixed at 0 degree in Celsius and stirred for 1 hour before raised to room temperature. | ||||
| COMMENT | |||||
| The PMID could not be found. | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000038 | ||||
Source |
J. Am. Chem. Soc. 1996, 118, 6826-6840 | ||||
Doi |
10.1021/ja952265x | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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