JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
 JCGG-RAC0000867
Submitter
 The Noguchi Institute
Reaction ID
 R-0000-000867
Regist Date
 2012/06/21 16:27:27
REACTANT
MOLECULE ID
 JCGG-COM0000984 (Reaction Tree)
Skeleton
JCGG-STR032134
Mol
 91 micro mole
MOLECULE ID
 JCGG-COM0000961 (Reaction Tree)
Mol
 90 micro mole
MOLECULE ID
 JCGG-COM0000578
Reactant Type
 HOBt
Mol
 99 micro mole
MOLECULE ID
 JCGG-COM0000704
Reactant Type
 NMM
Mol
 0.18 mmol
MOLECULE ID
 JCGG-COM0000946 (Reaction Tree)
Reactant Type
 EDC
Mol
 0.11 mmol
PRODUCT
MOLECULE ID
 JCGG-COM0001002 (Reaction Tree)
Yield
 58%
REACTION DETAIL
Reaction Time
 20 minutes, 12 hours
Reaction Temp
 -20 degree C, room temp
Solvent
 DMF, DMF
Comment
 1) +all reactants except EDC, 2) +EDC
COMMENT
The PMID could not be found.
There are two phases in this reaction.
REFERENCE
Reference Id
 REF-0000-000038
Source
 J. Am. Chem. Soc. 1996, 118, 6826-6840
Doi
 10.1021/ja952265x
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)