JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
 JCGG-RAC0000856
Submitter
 The Noguchi Institute
Reaction ID
 R-0000-000856
Regist Date
 2012/06/21 16:26:46
REACTANT
MOLECULE ID
 JCGG-COM0000984 (Reaction Tree)
Skeleton
JCGG-STR032134
Mol
 0.258 mmol
MOLECULE ID
 JCGG-COM0000985
Reactant Type
 N-Fmoc-gamma-(benzyloxy)threonine
Mol
 0.235 mmol
MOLECULE ID
 JCGG-COM0000578
Reactant Type
 HOBt
Mol
 0.356 mmol
MOLECULE ID
 JCGG-COM0000946 (Reaction Tree)
Reactant Type
 EDC
Mol
 0.308 mmol
PRODUCT
MOLECULE ID
 JCGG-COM0000986 (Reaction Tree)
Skeleton
JCGG-STR032134
Yield
 65%
REACTION DETAIL
Reaction Time
 20 minutes + 6 hours
Reaction Temp
 room temp
Solvent
 CH2Cl2
Comment
 The mixture was stirred for the initial 20 minutes at 0 degree in Celsius, and allowed to rise to room temperature within 6 hours.
COMMENT
The PMID could not be found.
ATTENTION: There is a typo in Experimental Section. (90 should be 92)
REFERENCE
Reference Id
 REF-0000-000038
Source
 J. Am. Chem. Soc. 1996, 118, 6826-6840
Doi
 10.1021/ja952265x
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)