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Glycan Syntheses |
JCGG ID |
JCGG-RAC0000853 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-000853
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Regist Date |
2012/06/21 16:26:36 | ||||
| REACTANT | |||||
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Reactant Type |
(phenylselenyl)proline derivative | ||||
Mol |
0.38 mmol | ||||
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Reactant Type |
pyridine | ||||
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Reactant Type |
H2O2 | ||||
| PRODUCT | |||||
MOLECULE ID |
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Product Type |
dehydro | ||||
Yield |
73% | ||||
| REACTION DETAIL | |||||
Reaction Time |
1 hour | ||||
Reaction Temp |
room temp | ||||
Solvent |
CH2Cl2 | ||||
Comment |
Initially, all reactants were cooled to 0 degree in Celsius, and gradually mixed. (approximately 1 hour) | ||||
| Pyridine was added dropwise. | |||||
| H2O2 was gradually added over a 5 min period. | |||||
| COMMENT | |||||
| The PMID could not be found. | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000038 | ||||
Source |
J. Am. Chem. Soc. 1996, 118, 6826-6840 | ||||
Doi |
10.1021/ja952265x | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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