JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
 JCGG-RAC0000849
Submitter
 The Noguchi Institute
Reaction ID
 R-0000-000849
Regist Date
 2012/06/21 16:26:21
REACTANT
MOLECULE ID
 JCGG-COM0000971 (Reaction Tree)
Skeleton
JCGG-STR032134
Reactant Type
 dissolved in 10% Pd/C in EtOAc/MeOH = (1/1)
MOLECULE ID
 JCGG-COM0000945 (Reaction Tree)
Reactant Type
 benzyl monoglutarate
MOLECULE ID
 JCGG-COM0000578
Reactant Type
 HOBt
MOLECULE ID
 JCGG-COM0000946 (Reaction Tree)
Reactant Type
 EDC
PRODUCT
MOLECULE ID
 JCGG-COM0000972 (Reaction Tree)
Skeleton
JCGG-STR032134
Yield
 54%
REACTION DETAIL
Reaction Time
 6 hours
Solvent
 CH2Cl2
Comment
 The procedure was the same as that described in Scheme 9.
90 was evaporated in Vacuo before the reaction. (2 hours)
The reaction temperature could not be found. (considered to be room temp)
COMMENT
The PMID could not be found.
REFERENCE
Reference Id
 REF-0000-000038
Source
 J. Am. Chem. Soc. 1996, 118, 6826-6840
Doi
 10.1021/ja952265x
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)