JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000848
Submitter
The Noguchi Institute
Reaction ID
R-0000-000848
Regist Date
2012/06/21 16:26:18
REACTANT
MOLECULE ID
JCGG-COM0000921 (Reaction Tree)
Skeleton
JCGG-STR032134
Reactant Type
dissolved in 30% TFA in CH2Cl2 (2 mL)
MOLECULE ID
JCGG-COM0000578
Reactant Type
HOBt
MOLECULE ID
JCGG-COM0000970 (Reaction Tree)
Reactant Type
N-Cbz-cis-3,4-di-hydroxy-D-proline
MOLECULE ID
JCGG-COM0000946 (Reaction Tree)
Reactant Type
EDC
MOLECULE ID
JCGG-COM0000047
Reactant Type
Et3N
PRODUCT
MOLECULE ID
JCGG-COM0000971 (Reaction Tree)
Skeleton
JCGG-STR032134
Yield
85%
REACTION DETAIL
Reaction Time
6 hours
Reaction Temp
room temp
Solvent
CH2Cl2
Comment
The procedure was the same as that described in Scheme 9.
COMMENT
The PMID could not be found.
REFERENCE
Reference Id
REF-0000-000038
Source
J. Am. Chem. Soc. 1996, 118, 6826-6840
Doi
10.1021/ja952265x

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)