JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
 JCGG-RAC0000846
Submitter
 The Noguchi Institute
Reaction ID
 R-0000-000846
Regist Date
 2012/06/21 16:26:11
REACTANT
MOLECULE ID
 JCGG-COM0000967 (Reaction Tree)
Skeleton
JCGG-STR032134
Reactant Type
 dissolved in 40% HNEt2 in THF (10 mL)
Mol
 0.27 mmol
MOLECULE ID
 JCGG-COM0000945 (Reaction Tree)
Reactant Type
 benzyl monoglutarate
Mol
 0.54 mmol
MOLECULE ID
 JCGG-COM0000578
Reactant Type
 HOBt
Mol
 0.54 mmol
MOLECULE ID
 JCGG-COM0000946 (Reaction Tree)
Reactant Type
 EDC
Mol
 0.54 mmol
PRODUCT
MOLECULE ID
 JCGG-COM0000968 (Reaction Tree)
Skeleton
JCGG-STR032134
Yield
 42%
REACTION DETAIL
Reaction Time
 10 hours
Reaction Temp
 0 degree C
Solvent
 THF
Comment
 88 was evaporated in Vacuo before the reaction. (2 hours)
COMMENT
The PMID could not be found.
REFERENCE
Reference Id
 REF-0000-000038
Source
 J. Am. Chem. Soc. 1996, 118, 6826-6840
Doi
 10.1021/ja952265x
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)