JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000841
Submitter
The Noguchi Institute
Reaction ID
R-0000-000841
Regist Date
2012/06/21 16:25:55
REACTANT
MOLECULE ID
JCGG-COM0000960 (Reaction Tree)
Mol
0.78 mmol
MOLECULE ID
JCGG-COM0000375
Reactant Type
PhCH(OMe)2
Mol
1.94 mmol
MOLECULE ID
JCGG-COM0000277
Reactant Type
CSA
Mol
0.78 mmol
MOLECULE ID
JCGG-COM0000649
Reactant Type
LiOH (0.25 N in MeOH/H2O)
PRODUCT
MOLECULE ID
JCGG-COM0000961 (Reaction Tree)
Yield
49%
REACTION DETAIL
Reaction Time
12 hours, 2 hours
Reaction Temp
60 degree C, room temp
Solvent
DMF, MeOH/H2O
Comment
1) 62+PhCH2(OMe)2, CSA, 2) +LiOH
COMMENT
The PMID could not be found.
REFERENCE
Reference Id
REF-0000-000038
Source
J. Am. Chem. Soc. 1996, 118, 6826-6840
Doi
10.1021/ja952265x

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)