JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000832
Submitter
The Noguchi Institute
Reaction ID
R-0000-000832
Regist Date
2012/06/21 16:25:25
REACTANT
MOLECULE ID
JCGG-COM0000945 (Reaction Tree)
Mol
3.43 mmol
MOLECULE ID
JCGG-COM0000047
Reactant Type
NEt3
Volume
0.2 mL
MOLECULE ID
JCGG-COM0000606
Reactant Type
DMF
Volume
0.5 mL
MOLECULE ID
JCGG-COM0000651
Reactant Type
NHS
Mol
3.43 mmol
MOLECULE ID
JCGG-COM0000946 (Reaction Tree)
Reactant Type
EDC
Mol
3.43 mmol
PRODUCT
MOLECULE ID
JCGG-COM0000947 (Reaction Tree)
Yield
71%
REACTION DETAIL
Reaction Time
2 hours
Reaction Temp
room temp
Solvent
CH2Cl2
Comment
The reactants were mixed at 0 degree in Celsius before stirred at room temperature.
COMMENT
The PMID could not be found.
REFERENCE
Reference Id
REF-0000-000038
Source
J. Am. Chem. Soc. 1996, 118, 6826-6840
Doi
10.1021/ja952265x

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)