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Glycan Syntheses |
JCGG ID |
JCGG-RAC0000831 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-000831
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Regist Date |
2012/06/21 16:25:22 | |||||||
| REACTANT | ||||||||
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Mol |
0.1 mmol | |||||||
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Reactant Type |
galactoside | |||||||
Mol |
0.15 mmol | |||||||
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Reactant Type |
TMSOTf | |||||||
Mol |
10 micro mole | |||||||
| PRODUCT | ||||||||
MOLECULE ID |
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Product Type |
alpha | |||||||
Yield |
58%(alpha/beta=84/16) | |||||||
MOLECULE ID |
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Product Type |
beta | |||||||
Yield |
58%(alpha/beta=84/16) | |||||||
| REACTION DETAIL | ||||||||
Reaction Time |
1 hour, 2 hours | |||||||
Reaction Temp |
room temp, -15 degree C | |||||||
Solvent |
CH2Cl2, CH2Cl2 | |||||||
Comment |
1) 57+galactoside, MS 4A, 2) +TMSOTf | |||||||
| COMMENT | ||||||||
| The PMID could not be found. | ||||||||
| There are two phases in this reaction. | ||||||||
| REFERENCE | ||||||||
Reference Id |
REF-0000-000038 | |||||||
Source |
J. Am. Chem. Soc. 1996, 118, 6826-6840 | |||||||
Doi |
10.1021/ja952265x | |||||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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