|
Glycan Syntheses |
JCGG ID |
JCGG-RAC0000826 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-000826
|
|||||||
Regist Date |
2012/06/21 16:25:08 | |||||||
| REACTANT | ||||||||
|
|
|
|
||||||
Mol |
0.858 mmol | |||||||
|
|
|
|||||||
Reactant Type |
BH3-NMe3 | |||||||
Mol |
5.15 mmol | |||||||
|
|
|
|||||||
Reactant Type |
AlCl3 | |||||||
Mol |
5.15 mmol | |||||||
| PRODUCT | ||||||||
MOLECULE ID |
|
|
|
|||||
Yield |
51% | |||||||
| REACTION DETAIL | ||||||||
Reaction Time |
30 minutes, 18 hours | |||||||
Reaction Temp |
room temp, room temp | |||||||
Solvent |
THF, THF | |||||||
Comment |
1) 39+BH3-NMe3, MS 4A, 2) +AlCl3 | |||||||
| Molecular sieves (4 A) was included in the solvent. | ||||||||
| COMMENT | ||||||||
| The PMID could not be found. | ||||||||
| There are two phases in this reaction. | ||||||||
| REFERENCE | ||||||||
Reference Id |
REF-0000-000038 | |||||||
Source |
J. Am. Chem. Soc. 1996, 118, 6826-6840 | |||||||
Doi |
10.1021/ja952265x | |||||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
|
