JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000823
Submitter
The Noguchi Institute
Reaction ID
R-0000-000823
Regist Date
2012/06/21 16:24:59
REACTANT
MOLECULE ID
JCGG-COM0000893 (Reaction Tree)
Mol
0.8 equiv.
MOLECULE ID
JCGG-COM0000894 (Reaction Tree)
Skeleton
JCGG-STR008276
Mol
1 equiv.
MOLECULE ID
JCGG-COM0000009
Reactant Type
Lewis Acid
Mol
0.5 equiv.
PRODUCT
MOLECULE ID
JCGG-COM0000895 (Reaction Tree)
Skeleton
JCGG-STR025272
Product Type
alpha
Yield
47%(alpha/beta=92/8)
MOLECULE ID
JCGG-COM0000896 (Reaction Tree)
Skeleton
JCGG-STR003547
Product Type
beta
Yield
47%(alpha/beta=92/8)
REACTION DETAIL
Reaction Time
1 hour
Reaction Temp
-15 degree C
Solvent
CH2Cl2
Comment
Molecular sieves (4 A) was included in the solvent.
COMMENT
The PMID could not be found.
REFERENCE
Reference Id
REF-0000-000038
Source
J. Am. Chem. Soc. 1996, 118, 6826-6840
Doi
10.1021/ja952265x

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)