|
Glycan Syntheses |
JCGG ID |
JCGG-RAC0000822 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-000822
|
|||||||
Regist Date |
2012/06/21 16:24:56 | |||||||
| REACTANT | ||||||||
|
|
|
|||||||
Mol |
0.8 equiv. | |||||||
|
|
|
|
||||||
Mol |
1 equiv. | |||||||
|
|
|
|||||||
Reactant Type |
Lewis Acid | |||||||
Mol |
0.05 equiv. | |||||||
| PRODUCT | ||||||||
MOLECULE ID |
|
|
|
|||||
Product Type |
alpha | |||||||
Yield |
68%(alpha/beta=92/8) | |||||||
MOLECULE ID |
|
|
|
|||||
Product Type |
beta | |||||||
Yield |
68%(alpha/beta=92/8) | |||||||
| REACTION DETAIL | ||||||||
Reaction Time |
1 hour | |||||||
Reaction Temp |
-15 degree C | |||||||
Solvent |
CH2Cl2 | |||||||
Comment |
Molecular sieves (4 A) was included in the solvent. | |||||||
| COMMENT | ||||||||
| The PMID could not be found. | ||||||||
| REFERENCE | ||||||||
Reference Id |
REF-0000-000038 | |||||||
Source |
J. Am. Chem. Soc. 1996, 118, 6826-6840 | |||||||
Doi |
10.1021/ja952265x | |||||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
|
