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Glycan Syntheses |
JCGG ID |
JCGG-RAC0000800 | |||||||
Submitter |
The Noguchi Institute | |||||||
Reaction ID |
R-0000-000800
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Regist Date |
2012/06/21 16:23:56 | |||||||
| REACTANT | ||||||||
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Reactant Type |
Donor Phosphite | |||||||
| id=12 (alpha) | ||||||||
Mol |
0.76 equiv. | |||||||
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Reactant Type |
Donor Phosphite | |||||||
| id=12 (beta) | ||||||||
Mol |
0.24 equiv. | |||||||
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Reactant Type |
TMSOTf | |||||||
Mol |
0.5 equiv. | |||||||
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Reactant Type |
TMB | |||||||
Mol |
2 equiv. | |||||||
| PRODUCT | ||||||||
MOLECULE ID |
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Yield |
77% | |||||||
| REACTION DETAIL | ||||||||
Reaction Time |
1 hour | |||||||
Reaction Temp |
-15 degree C | |||||||
Solvent |
CH2Cl2 | |||||||
Comment |
Molecular sieves (3 A) was included in the solvent. | |||||||
| COMMENT | ||||||||
| The PMID could not be found. | ||||||||
| REFERENCE | ||||||||
Reference Id |
REF-0000-000038 | |||||||
Source |
J. Am. Chem. Soc. 1996, 118, 6826-6840 | |||||||
Doi |
10.1021/ja952265x | |||||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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