JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
 JCGG-RAC0000791
Submitter
 The Noguchi Institute
Reaction ID
 R-0000-000791
Regist Date
 2012/06/21 16:23:31
REACTANT
MOLECULE ID
 JCGG-COM0000868 (Reaction Tree)
Reactant Type
 Donor Phosphite
Mol
 1 equiv.
MOLECULE ID
 JCGG-COM0000201
Reactant Type
 TMB
Mol
 2 equiv.
MOLECULE ID
 JCGG-COM0000009
Reactant Type
 TMSOTf
Mol
 0.5 equiv.
PRODUCT
MOLECULE ID
 JCGG-COM0000869 (Reaction Tree)
Yield
 68%
REACTION DETAIL
Reaction Time
 1 hour
Reaction Temp
 -78 degree C
Solvent
 CH2Cl2
Comment
 Molecular sieves (3 A) was included in the solvent.
COMMENT
The PMID could not be found.
REFERENCE
Reference Id
 REF-0000-000038
Source
 J. Am. Chem. Soc. 1996, 118, 6826-6840
Doi
 10.1021/ja952265x
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)