JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
 JCGG-RAC0000771
Submitter
 The Noguchi Institute
Reaction ID
 R-0000-000775
Regist Date
 2012/06/21 16:22:51
REACTANT
MOLECULE ID
 JCGG-COM0000358 (Reaction Tree)
Reactant Type
 1-C-Alkyl-hexopyranose
Mol
 1 equiv.
MOLECULE ID
 JCGG-COM0000111
Reactant Type
 Brφnsted acid
Mol
 0.05 equiv.
PRODUCT
MOLECULE ID
 JCGG-COM0000359 (Reaction Tree)
Product Type
 id=2e/5e = 1C4/boat
Yield
 70%/26% = 2e/5e
REACTION DETAIL
Reaction Time
 2 hours
Reaction Temp
 0 degree C
Solvent
 MeCN
Comment
 Dry MgSO4 was included in the solvent.
COMMENT
The PMID could not be found.
REFERENCE
Reference Id
 REF-0000-000037
Source
 SYNLETT 2005, No. 19, pp 2973-2977
Doi
 10.1055/s-2005-921912
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