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Glycan Syntheses |
JCGG ID |
JCGG-RAC0000722 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-000722
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Regist Date |
2012/06/21 16:20:16 | ||||
| REACTANT | |||||
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Reactant Type |
1-C-Methylated donor | ||||
Mol |
1 equiv. | ||||
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Reactant Type |
Aldopyranose of acceptor | ||||
Mol |
0.67 equiv. | ||||
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Reactant Type |
Activator | ||||
Mol |
0.05 equiv. | ||||
| PRODUCT | |||||
MOLECULE ID |
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Product Type |
alpha | ||||
Yield |
80%(alpha/beta=100/0) | ||||
| REACTION DETAIL | |||||
Reaction Time |
3 hours | ||||
Reaction Temp |
0 degree C | ||||
Solvent |
CH2Cl2 | ||||
Catalyst |
Activator | ||||
Comment |
CaSO4 was included in the solvent. | ||||
| COMMENT | |||||
| The PMID could not be found. | |||||
| Only alpha was obtained. | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000034 | ||||
Source |
Tetrahedron: Asymmetry 17 (2006) 2914-2918 | ||||
Doi |
10.1016/j.tetasy.2006.11.008 | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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