Reaction:JCGG-RAC0000720

JCGG ID		JCGG-RAC0000720
Submitter		The Noguchi Institute
Reaction ID		R-0000-000720
Regist Date		2012/06/21 16:20:10
REACTANT
MOLECULE ID		JCGG-COM0000085 (Reaction Tree)
	Reactant Type	1-C-Methylated donor
	Mol	1 equiv.
MOLECULE ID		JCGG-COM0000303 (Reaction Tree)
	Reactant Type	Aldopyranose of acceptor
	Mol	0.67 equiv.
MOLECULE ID		JCGG-COM0000231
	Reactant Type	Activator
	Mol	0.05 equiv.
PRODUCT
MOLECULE ID		JCGG-COM0000348 (Reaction Tree)
	Product Type	alpha
	Yield	89%(alpha/beta=76/24)
MOLECULE ID		JCGG-COM0000349 (Reaction Tree)
	Product Type	beta
	Yield	89%(alpha/beta=76/24)
REACTION DETAIL
Reaction Time		3 hours
Reaction Temp		0 degree C
Solvent		CH2Cl2
Catalyst		Activator
Comment		CaSO4 was included in the solvent.
COMMENT
The PMID could not be found.
REFERENCE
Reference Id		REF-0000-000034
	Source	Tetrahedron: Asymmetry 17 (2006) 2914-2918
	Doi	10.1016/j.tetasy.2006.11.008