JCGG ID |
JCGG-RAC0000677 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-000677
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Regist Date |
2012/06/21 16:18:10 | ||||
| REACTANT | |||||
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Mol |
1 equiv. | ||||
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Reactant Type |
O3 | ||||
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Reactant Type |
Ph3P | ||||
Mol |
5 equiv. | ||||
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Reactant Type |
NaBH4 | ||||
Mol |
8 equiv. | ||||
| PRODUCT | |||||
MOLECULE ID |
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Yield |
72% | ||||
| REACTION DETAIL | |||||
Reaction Time |
45 minutes, 3 hours | ||||
Reaction Temp |
-78 degree C, 0 degree C | ||||
Solvent |
CH2Cl2, THF | ||||
Catalyst |
Ph3P, NaBH4 | ||||
Comment |
1) 12+O3, Ph3P, 2) NaBH4 | ||||
| COMMENT | |||||
| The PMID could not be found. | |||||
| There are two phases in this reaction. | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000032 | ||||
Source |
Tetrahedron Letters 48 (2007) 5807-5810 | ||||
Doi |
10.1016/j.tetlet.2007.06.057 | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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