JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000677
Submitter
The Noguchi Institute
Reaction ID
R-0000-000677
Regist Date
2012/06/21 16:18:10
REACTANT
MOLECULE ID
JCGG-COM0000775 (Reaction Tree)
Mol
1 equiv.
MOLECULE ID
JCGG-COM0000484
Reactant Type
O3
MOLECULE ID
JCGG-COM0000408
Reactant Type
Ph3P
Mol
5 equiv.
MOLECULE ID
JCGG-COM0000776
Reactant Type
NaBH4
Mol
8 equiv.
PRODUCT
MOLECULE ID
JCGG-COM0000777 (Reaction Tree)
Yield
72%
REACTION DETAIL
Reaction Time
45 minutes, 3 hours
Reaction Temp
-78 degree C, 0 degree C
Solvent
CH2Cl2, THF
Catalyst
Ph3P, NaBH4
Comment
1) 12+O3, Ph3P, 2) NaBH4
COMMENT
The PMID could not be found.
There are two phases in this reaction.
REFERENCE
Reference Id
REF-0000-000032
Source
Tetrahedron Letters 48 (2007) 5807-5810
Doi
10.1016/j.tetlet.2007.06.057

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)