JCGG ID |
JCGG-RAC0000677 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-000677 | ||||
Regist Date |
2012/06/21 16:18:10 | ||||
REACTANT | |||||
|
|
||||
Mol |
1 equiv. | ||||
|
|
||||
Reactant Type |
O3 | ||||
|
|
||||
Reactant Type |
Ph3P | ||||
Mol |
5 equiv. | ||||
|
|
||||
Reactant Type |
NaBH4 | ||||
Mol |
8 equiv. | ||||
PRODUCT | |||||
MOLECULE ID |
|
|
|||
Yield |
72% | ||||
REACTION DETAIL | |||||
Reaction Time |
45 minutes, 3 hours | ||||
Reaction Temp |
-78 degree C, 0 degree C | ||||
Solvent |
CH2Cl2, THF | ||||
Catalyst |
Ph3P, NaBH4 | ||||
Comment |
1) 12+O3, Ph3P, 2) NaBH4 | ||||
COMMENT | |||||
The PMID could not be found. | |||||
There are two phases in this reaction. | |||||
REFERENCE | |||||
Reference Id |
REF-0000-000032 | ||||
Source |
Tetrahedron Letters 48 (2007) 5807-5810 | ||||
Doi |
10.1016/j.tetlet.2007.06.057 |
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST) |