JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
 JCGG-RAC0000672
Submitter
 The Noguchi Institute
Reaction ID
 R-0000-000672
Regist Date
 2012/06/21 16:17:57
REACTANT
MOLECULE ID
 JCGG-COM0000766 (Reaction Tree)
Mol
 1 equiv.
MOLECULE ID
 JCGG-COM0000161
Reactant Type
 BnBr
Mol
 1.5 equiv.
MOLECULE ID
 JCGG-COM0000160
Reactant Type
 NaH
Mol
 4 equiv.
PRODUCT
MOLECULE ID
 JCGG-COM0000767 (Reaction Tree)
Yield
 96%
REACTION DETAIL
Reaction Time
 overnight
Reaction Temp
 room temp
Solvent
 DMF
Comment
 The reactants were mixed at 0 degree in Celsius before stirred at room temperature.
COMMENT
The PMID could not be found.
REFERENCE
Reference Id
 REF-0000-000032
Source
 Tetrahedron Letters 48 (2007) 5807-5810
Doi
 10.1016/j.tetlet.2007.06.057
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)