JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000669
Submitter
The Noguchi Institute
Reaction ID
R-0000-000669
Regist Date
2012/06/21 16:17:49
REACTANT
MOLECULE ID
JCGG-COM0000760 (Reaction Tree)
Skeleton
JCGG-STR032527
Mol
1 equiv.
MOLECULE ID
JCGG-COM0000761
Reactant Type
Tf2O
Mol
1.5 equiv.
PRODUCT
MOLECULE ID
JCGG-COM0000762 (Reaction Tree)
Skeleton
JCGG-STR032527
Yield
93%
REACTION DETAIL
Reaction Time
2.5 hours
Reaction Temp
room temp
Solvent
pyridine
Comment
The reactants were mixed at -20 degree in Celsius before stirred at room temperature.
COMMENT
The PMID could not be found.
REFERENCE
Reference Id
REF-0000-000032
Source
Tetrahedron Letters 48 (2007) 5807-5810
Doi
10.1016/j.tetlet.2007.06.057

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)