JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000664
Submitter
The Noguchi Institute
Reaction ID
R-0000-000664
Regist Date
2012/06/21 16:17:34
REACTANT
MOLECULE ID
JCGG-COM0000751 (Reaction Tree)
Reactant Type
imino ether
Mol
0.001 mmol
MOLECULE ID
JCGG-COM0000412
Reactant Type
TBAI
Weight
5 mg (and more)
PRODUCT
MOLECULE ID
JCGG-COM0000750 (Reaction Tree)
Yield
40%
REACTION DETAIL
Reaction Time
overnight
Solvent
THF
Comment
Amberlite IR-120 was included in the solvent.
COMMENT
REFERENCE
Reference Id
REF-0000-000030
Issn
Print
PubMed ID
10813908
Journal Name
The Journal of organic chemistry. (2000) 65 (1): 144-51.
Article Title
A total synthesis of the methyl glycoside of ganglioside GM(1).
Author
S K, Bhattacharya; S J, Danishefsky
Affiliation
Department of Chemistry, Columbia University, Havemeyer Hall, New York, New York 10027, USA.
Reference Id
REF-0000-000031
Source
J. Org. Chem., 2000, 65, 144-151
Doi
10.1021/jo9912496

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)