JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000660
Submitter
The Noguchi Institute
Reaction ID
R-0000-000660
Regist Date
2012/06/21 16:17:22
REACTANT
MOLECULE ID
JCGG-COM0000742 (Reaction Tree)
Reactant Type
tetrasaccharide
Mol
0.02 mmol
MOLECULE ID
JCGG-COM0000743
Reactant Type
DDQ
Mol
0.051 mmol
PRODUCT
MOLECULE ID
JCGG-COM0000744 (Reaction Tree)
Yield
51%
REACTION DETAIL
Reaction Time
2 hours
Solvent
CH2Cl2/H2O = 1mL/0.06mL
Comment
The reaction temperature could not be found. (considered to be room temp)
COMMENT
REFERENCE
Reference Id
REF-0000-000030
Issn
Print
PubMed ID
10813908
Journal Name
The Journal of organic chemistry. (2000) 65 (1): 144-51.
Article Title
A total synthesis of the methyl glycoside of ganglioside GM(1).
Author
S K, Bhattacharya; S J, Danishefsky
Affiliation
Department of Chemistry, Columbia University, Havemeyer Hall, New York, New York 10027, USA.
Reference Id
REF-0000-000031
Source
J. Org. Chem., 2000, 65, 144-151
Doi
10.1021/jo9912496

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)