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Glycan Syntheses |
JCGG ID |
JCGG-RAC0000607 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-000607
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Regist Date |
2012/06/21 16:14:49 | ||||
| REACTANT | |||||
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Mol |
18.83 mmol | ||||
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Reactant Type |
MsOH | ||||
Mol |
46.25 mmol | ||||
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Reactant Type |
BnOCH2COONSu | ||||
Mol |
23.78 mmol | ||||
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Reactant Type |
TEA | ||||
Volume |
4mL | ||||
| PRODUCT | |||||
MOLECULE ID |
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Yield |
75% | ||||
| REACTION DETAIL | |||||
Reaction Time |
24 hours, 24 hours | ||||
Reaction Temp |
60 degree C, room temp | ||||
Solvent |
dry MeOH, CH3CN/H2O = 15/1 | ||||
Comment |
1) 3+MsOH, 2) +BnOCH2COONSu, TEA | ||||
| COMMENT | |||||
| There are two phases in this reaction. | |||||
| The product was used for the next reaction. | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000028 | ||||
Issn |
Electronic | ||||
Doi |
10.1021/jm8000696 | ||||
PubMed ID |
18841881 | ||||
Journal Name |
Journal of medicinal chemistry. (2008) 51 (21): 6665-81. | ||||
Article Title |
Design, synthesis, and structure-affinity relationships of novel series of sialosides as CD22-specific inhibitors. | ||||
Author |
Hajjaj H M, Abdu-Allah; Taichi, Tamanaka; Jie, Yu; Lu, Zhuoyuan; Magesh, Sadagopan; Takahiro, Adachi; Takeshi, Tsubata; Soerge, Kelm; Hideharu, Ishida; Makoto, Kiso | ||||
Affiliation |
Department of Applied Bio-organic Chemistry, The United Graduate School of Agricultural Sciences, Gifu University, Gifu 501-1193, Japan. | ||||
Reference Id |
REF-0000-000029 | ||||
Source |
J. Med. Chem., 2008, 51, 6665-6681 | ||||
Doi |
10.1021/jm8000696 | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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