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Glycan Syntheses |
JCGG ID |
JCGG-RAC0000591 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-000591
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Regist Date |
2012/06/21 16:13:59 | ||||
| REACTANT | |||||
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Mol |
0.130 mmol | ||||
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Reactant Type |
(ClCO)2 | ||||
Mol |
392 micro mole | ||||
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Reactant Type |
DMF | ||||
Mol |
2.61 mmol | ||||
| PRODUCT | |||||
MOLECULE ID |
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Yield |
98% | ||||
| REACTION DETAIL | |||||
Reaction Time |
3 hours | ||||
Reaction Temp |
room temp | ||||
Solvent |
CH2Cl2/DMF = 1.3mL/201microL | ||||
Comment |
Vilsmeier's reagent was generated by the reaction between DMF and (ClCO)2 | ||||
| COMMENT | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000026 | ||||
Issn |
|||||
Doi |
10.1021/ol051592z | ||||
PubMed ID |
16178547 | ||||
Journal Name |
Organic letters. (2005) 7 (20): 4415-8. | ||||
Article Title |
Di-tert-butylsilylene-directed alpha-selective synthesis of 4-methylumbelliferyl T-antigen. | ||||
Author |
Akihiro, Imamura; Hiromune, Ando; Hideharu, Ishida; Makoto, Kiso | ||||
Affiliation |
Department of Applied Bioorganic Chemistry, Gifu University, Gifu 501-1193, Japan. | ||||
Reference Id |
REF-0000-000027 | ||||
Source |
ORGANIC LETTERS, 2005, Vol. 7, No. 20, 4415-4418 | ||||
Doi |
10.1021/ol051592z | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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