JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000588
Submitter
The Noguchi Institute
Reaction ID
R-0000-000588
Regist Date
2012/06/21 16:13:52
REACTANT
MOLECULE ID
JCGG-COM0000497 (Reaction Tree)
Mol
5.59 mmol
MOLECULE ID
JCGG-COM0000599
Reactant Type
DTBS(OTf)2
Mol
6.15 mmol
PRODUCT
MOLECULE ID
JCGG-COM0000600 (Reaction Tree)
Yield
93%
REACTION DETAIL
Reaction Time
5 minutes
Reaction Temp
room temp
Solvent
pyridine
Catalyst
DTBS(OTf)2
COMMENT
REFERENCE
Reference Id
REF-0000-000026
Issn
Print
Doi
10.1021/ol051592z
PubMed ID
16178547
Journal Name
Organic letters. (2005) 7 (20): 4415-8.
Article Title
Di-tert-butylsilylene-directed alpha-selective synthesis of 4-methylumbelliferyl T-antigen.
Author
Akihiro, Imamura; Hiromune, Ando; Hideharu, Ishida; Makoto, Kiso
Affiliation
Department of Applied Bioorganic Chemistry, Gifu University, Gifu 501-1193, Japan.
Reference Id
REF-0000-000027
Source
ORGANIC LETTERS, 2005, Vol. 7, No. 20, 4415-4418
Doi
10.1021/ol051592z

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)