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Glycan Syntheses |
JCGG ID |
JCGG-RAC0000560 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-000560
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Regist Date |
2012/06/21 16:12:37 | ||||
| REACTANT | |||||
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Mol |
16.6 micro mole | ||||
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Reactant Type |
HBTU | ||||
Mol |
50 micro mole | ||||
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Reactant Type |
HOBt | ||||
Mol |
50 micro mole | ||||
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Reactant Type |
Ac2O | ||||
Volume |
1.5 mL | ||||
| PRODUCT | |||||
MOLECULE ID |
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Yield |
76.2% | ||||
| REACTION DETAIL | |||||
Reaction Time |
4 hours, 12 hours | ||||
Reaction Temp |
65 degree C, room temp | ||||
Solvent |
DMF, pyridine | ||||
Comment |
1) 9+HBTU+HOBt, 2) +Ac2O | ||||
| COMMENT | |||||
| The PMID could not be found. | |||||
| There are two phases in this reaction. | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000024 | ||||
Source |
JOURNAL OF CARBOHYDRATE CHEMISTRY, Vol. 23, No. 4, pp. 201-215, 2004 | ||||
Doi |
10.1081/CAR-200030039 | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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