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Glycan Syntheses |
JCGG ID |
JCGG-RAC0000544 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-000545
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Regist Date |
2012/06/21 16:11:55 | ||||
| REACTANT | |||||
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Mol |
49.1 mmol | ||||
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Mol |
32.8 mmol | ||||
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Reactant Type |
NIS | ||||
Mol |
54.2 mmol | ||||
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Reactant Type |
TMSOTf | ||||
Mol |
4.92 mmol | ||||
| PRODUCT | |||||
MOLECULE ID |
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Yield |
74.9%(at least) | ||||
| REACTION DETAIL | |||||
Reaction Time |
30 minutes | ||||
Reaction Temp |
-40 degree C | ||||
Solvent |
CH2Cl2 | ||||
Catalyst |
NIS, TMSOTf | ||||
| COMMENT | |||||
| The PMID could not be found. | |||||
| The product was used for the next reaction. (without purification) | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000023 | ||||
Source |
Journal of Carbohydrate Chemistry, 17: 4, 729 - 738 | ||||
Doi |
10.1080/07328309808002348 | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
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