JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000502
Submitter
The Noguchi Institute
Reaction ID
R-0000-000503
Regist Date
2012/06/21 16:09:41
REACTANT
MOLECULE ID
JCGG-COM0000085 (Reaction Tree)
Reactant Type
Ketose
Mol
1 equiv.
MOLECULE ID
JCGG-COM0000046 (Reaction Tree)
Reactant Type
Aldose
Mol
0.67 equiv.
MOLECULE ID
JCGG-COM0000113
Reactant Type
Activator
Mol
0.05 equiv.
PRODUCT
MOLECULE ID
JCGG-COM0000344 (Reaction Tree)
Product Type
alpha
Yield
47%
REACTION DETAIL
Reaction Time
3 hours
Reaction Temp
0 degree C
Solvent
MeCN
Catalyst
Activator
Comment
CaSO4 was added to the solvent as a drying agent.
COMMENT
The PMID could not be found.
Only alpha was obtained.
The structure of the product (#41) may be wrong.
REFERENCE
Reference Id
REF-0000-000009
Source
HETEROCYCLES, Vol. 79, 2009, pp. 163 - 194
Doi
10.3987/REV-08-SR(D)4

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)