JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
 JCGG-RAC0000487
Submitter
 The Noguchi Institute
Reaction ID
 R-0000-000488
Regist Date
 2012/06/21 16:08:56
REACTANT
MOLECULE ID
 JCGG-COM0000006
Reactant Type
 activator
Mol
 0.05 equiv.
MOLECULE ID
 JCGG-COM0000452 (Reaction Tree)
Reactant Type
 glycosyl donor
Mol
 1 equiv.
MOLECULE ID
 JCGG-COM0000046 (Reaction Tree)
Reactant Type
 Acceptor
Mol
 0.5 equiv.
PRODUCT
MOLECULE ID
 JCGG-COM0000465 (Reaction Tree)
Product Type
 alpha+alpha
Yield
 80%(alpha+alpha/alpha+beta/beta+alpha/beta+beta=20/8/28/44)
MOLECULE ID
 JCGG-COM0000466 (Reaction Tree)
Product Type
 alpha+beta
Yield
 80%(alpha+alpha/alpha+beta/beta+alpha/beta+beta=20/8/28/44)
MOLECULE ID
 JCGG-COM0000467 (Reaction Tree)
Product Type
 beta+alpha
Yield
 80%(alpha+alpha/alpha+beta/beta+alpha/beta+beta=20/8/28/44)
MOLECULE ID
 JCGG-COM0000468 (Reaction Tree)
Product Type
 beta+beta
Yield
 80%(alpha+alpha/alpha+beta/beta+alpha/beta+beta=20/8/28/44)
REACTION DETAIL
Reaction Time
 3 hours
Reaction Temp
 room temp
Solvent
 CH2Cl2
Catalyst
 activator
Comment
 CaSO4 was added to the solvent as a drying agent.
COMMENT
The PMID could not be found.
REFERENCE
Reference Id
 REF-0000-000020
Source
 HETEROCYCLES, Vol. 81, No. 5, 2010, pp. -
Doi
 10.3987/COM-10-11916
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)