JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000482
Submitter
The Noguchi Institute
Reaction ID
R-0000-000483
Regist Date
2012/06/21 16:08:41
REACTANT
MOLECULE ID
JCGG-COM0000452 (Reaction Tree)
Reactant Type
glycosyl donor
Mol
1 equiv.
MOLECULE ID
JCGG-COM0000096
Reactant Type
Acceptor
Mol
1 equiv.
MOLECULE ID
JCGG-COM0000006
Reactant Type
activator
Mol
0.05 equiv.
PRODUCT
MOLECULE ID
JCGG-COM0000459 (Reaction Tree)
Product Type
alpha
Yield
81%(alpha/beta=32/68)
MOLECULE ID
JCGG-COM0000460 (Reaction Tree)
Product Type
beta
Yield
81%(alpha/beta=32/68)
REACTION DETAIL
Reaction Time
3 hours
Reaction Temp
room temp
Solvent
CH2Cl2
Catalyst
activator
Comment
CaSO4 was added to the solvent as a drying agent.
COMMENT
The PMID could not be found.
REFERENCE
Reference Id
REF-0000-000020
Source
HETEROCYCLES, Vol. 81, No. 5, 2010, pp. -
Doi
10.3987/COM-10-11916

©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)