JCGGDB TOP Glycan Syntheses

Reaction

JCGG ID
JCGG-RAC0000480
Submitter
The Noguchi Institute
Reaction ID
R-0000-000481
Regist Date
2012/06/21 16:08:35
REACTANT
MOLECULE ID
JCGG-COM0000452 (Reaction Tree)
Reactant Type
glycosyl donor
Mol
1 equiv.
MOLECULE ID
JCGG-COM0000046 (Reaction Tree)
Reactant Type
Acceptor
Mol
0.5 equiv.
MOLECULE ID
JCGG-COM0000006
Reactant Type
activator
Mol
0.05 equiv.
PRODUCT
MOLECULE ID
JCGG-COM0000456 (Reaction Tree)
Product Type
alpha
Yield
88%(alpha/beta=65/35)
MOLECULE ID
JCGG-COM0000457 (Reaction Tree)
Product Type
beta
Yield
88%(alpha/beta=65/35)
REACTION DETAIL
Reaction Time
3 hours
Reaction Temp
room temp
Solvent
PhMe
Catalyst
activator
Comment
CaSO4 was added to the solvent as a drying agent.
COMMENT
The PMID could not be found.
REFERENCE
Reference Id
REF-0000-000020
Source
HETEROCYCLES, Vol. 81, No. 5, 2010, pp. -
Doi
10.3987/COM-10-11916

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