|
Glycan Syntheses |
JCGG ID |
JCGG-RAC0000474 | ||||
Submitter |
The Noguchi Institute | ||||
Reaction ID |
R-0000-000475
|
||||
Regist Date |
2012/06/21 16:08:19 | ||||
| REACTANT | |||||
|
|
|
||||
Reactant Type |
ketopyranose | ||||
Mol |
1 equiv. | ||||
|
|
|
||||
Reactant Type |
Brφnsted acid | ||||
Mol |
0.05 equiv. | ||||
| PRODUCT | |||||
MOLECULE ID |
|
|
|||
Product Type |
anhydroketopyranose | ||||
Yield |
96%(1C4/boat=70/26) | ||||
| REACTION DETAIL | |||||
Reaction Time |
2 hours | ||||
Reaction Temp |
0 degree C | ||||
Solvent |
MeCN | ||||
Catalyst |
Brφnsted acid | ||||
Comment |
CaSO4 was added to the solvent as a drying agent. | ||||
| COMMENT | |||||
| The PMID could not be found. | |||||
| REFERENCE | |||||
Reference Id |
REF-0000-000019 | ||||
Source |
HETEROCYCLES, Vol. 82, No. 1, 2010, pp. - | ||||
Doi |
10.3987/COM-10-S(E)24 | ||||
©2008-2013 Research Center for Medical Glycoscience, National Institute of Advanced Industrial Science and Technology (AIST)
|